The graphene production equipment for the high-end intelligent equipment preparation method of graphene is a high-tech advanced equipment for single-layer, multi-layer and other high-quality graphene produced by mechanical hydraulic shearing and cavitation stripping of graphite sheets. The invention and application of this advanced technology have accelerated the pace of graphene production to a certain extent, and also promoted the confidence of graphene production enterprises in large-scale, high-efficiency, low-cost, pollution-free production. Moreover, the production process of the mechanical hydraulic shearing and cavitation vortex stripping graphite sheet has the characteristics of simple operation, safety and reliability, no oxidation, no high temperature, high quality and high quality, and is very suitable for mass production of high quality graphene.

[Device Structure]

The main equipment structure of graphene production equipment is high-end intelligent equipment integrated control system of graphene, high shear dispersing mixing batching tank, fine dispersion grinding unit (sodium meter cone grinding), hydraulic vortex cavitation, high shearing Flow ultrasonic device, multi-pipe condenser, ultrasonic storage tank, pressure gauge temperature controller and so on.

【working principle】

Graphene grinding and dispersing machine is a high-end discrete peeling and grinding nano-cone grinding intelligent equipment preparation. The main working principle is a new type of nano-scale dispersion colloid mill. The intelligently controlled stripping mechanical multi-function grinding machine principle is also called high-end intelligence of graphene. Equipment preparation method, its advanced high-end intelligent nano graphene production equipment. The graphene production equipment is added with graphite powder, dispersant or surface modifier and water in a high-speed dispersing and stirring storage tank, and then dispersed and stirred by a high-speed disperser to prepare a graphite solution with good dispersion stability. The pipe enters the finely dispersed grinding chamber through a special pulverizing and cutting and peeling device, and the particles, the brittle mass, the agglomerate and the like in the graphite solution are rapidly dispersed and sheared, and then sucked into the third-stage refining zone and the high shear cutting The area of ​​shear pulverization and delamination structure in the area, in the very narrow working aisle, due to the rapid cutting of thousands of sets of moving and static grinding slots and thousands of pairs of shearing blades and shearing blades, resulting in strong friction and Disperse, cut, peel, depolymerize, pulverize, grind, etc. Under the action of mechanical motion and centrifugal force, the stripped graphite is pressed into the cutting and stripping zone for grinding and crushing. The fine grinding distinguishes three grades. The more outwardly, the higher the precision of the first-stage grinding disc, the smaller the pitch, the higher the linear velocity. Long, the more the graphite sheet is peeled off, and the fluid gradually curves toward the radial direction. The velocity of the fluid in each stage changes instantaneously, and is subjected to tens of millions of high-speed shears per minute, strong friction, extrusion grinding, particle pulverization, etc., after passing through the three-stage refining zone and the high-shear cutting zone. After tens of millions of high-speed shearing, grinding and pulverizing, graphite strand molecular chain breakage, sheet cutting tearing, and the like are produced. Then through the high pressure pipe into the hydraulic vortex shear cavitation generator; hydraulic vortex shear cavitation technology is a process in which the graphite solution flows into the vortex low pressure region to form vapor vacuoles, when the internal pressure of the graphite solution is reduced to saturated vapor When the pressure is below, the bubbles formed by the hydraulic shear cavitation process begin to appear and grow, and as time passes, the bubbles expand, grow, compress and collapse. But this process is sexual, less than a thousand and six seconds, the bubble can release huge energy at the moment of rapid collapse, instantaneous local high temperature (1900-5000K) and high pressure (up to 140Mpa-170Mpa), and the speed is about It is a micro-jet with a strong impact force of 50-110 m/s, thus causing a series of phenomena such as cavitation, air noise, vibration and luminescence. The effects of cavitation are usually called hydraulic vortex shear cavitation effects. The graphite sheet is peeled off from the monolayer and multilayer ideal graphene products.

[Process Flow]

First, the graphene production equipment is equipped with a graphite powder, a dispersant or a surface modifier and water for mixing and stirring in a high-shear dispersing mill with a mixing tank, first closing the circulation valve and then opening the storage tank to connect with the dispersion grinding pump. The valve allows the graphite solution to pass through a fine dispersion grinder, a hydraulic shear vortex cavitation and then enter the high shear cyclone ultrasonic hopper through pressure. When the batching tank is empty, the lower connecting valve is automatically closed and the circulation valve is opened to allow the graphite solution to continuously unravel from the circulation to make the graphene single layer multi-layered to the desired effect, and the pressure control, time control and temperature control are designed in the integrated control system. You can also use computer control or touch frequency control or fully automatic control.

[equipment advantage]

  Wenzhou Haoxing Machinery Equipment Manufacturing Co., Ltd. develops graphene grinding machine, which is a high-end intelligent graphene equipment-nano colloid mill-dispersion peeling grinder with its own patented technology. It adopts physical stripping method and retains the characteristics of pure graphene to a large extent. And applied to Guizhou Dingsheng Ethylene High-Tech Co., Ltd. is the first manufacturer in China with an annual output of 100 tons of graphene and a second-phase annual output of 400 tons of graphene with a production value of 50 billion yuan. It can be customized according to customer needs, different specifications and The graphene powder used in the application and the lithium battery conductive agent of the slurry company have been successfully introduced into many large-scale lithium battery enterprises and coated aluminum foil enterprises in China as positive electrode conductive agents, negative electrode conductive agents and carbon coated aluminum foil pastes. The company's high thermal conductivity carbon-plastic alloy material is the material of choice for replacing metal aluminum heat sinks with excellent thermal conductivity. The graphite crucible re-enters the new hydraulic shear cavitation cyclone ultrasonic generator through the pipeline, so that the graphite solution is subjected to the cyclone cavitation ultrasonic wave in the high-speed jet shear shock and slow grinding space of the comet nanometer cone mill. The graphite layer is not subjected to cyclic cutting and stripping to produce high-quality single-layer and multi-layer graphene into the storage tank, and then re-enters the fine dispersing machine and the hydraulic vortex cavitation device through the condenser return line, graphite The entire cutting and stripping process of the olefin solution is subjected to intense cutting and uninterrupted peeling under the effects of high-speed impact cutting, hydraulic shear vortex cavitation, and swirling ultrasonic cavitation in a closed pipeline. Better quality single-layer and multi-layer graphene, this mechanical hydraulic cavitation stripping graphene process can strongly promote and promote the large-scale, high-efficiency, low-cost, pollution-free production of graphene.